4-Dimethylaminobenzaldehyde synthesis
- Product Name:4-Dimethylaminobenzaldehyde
- CAS Number:100-10-7
- Molecular formula:C9H11NO
- Molecular Weight:149.19
31362-12-6
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100-10-7
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Yield:100-10-7 95%
Reaction Conditions:
with iodosylbenzene in dichloromethane at 20; for 0.25 h;
Steps:
General procedure for the deprotection process.
General procedure: To a solution of 1,3-dithiolane/dithiane (2.0 mmol) in DCM (5.0 mL) was added the well ground PhIO (2.4 mmol) powder with stirring. The mixture was stirred at room temperature until TLC revealed a complete consumption of the substrates. Then the reaction solution was concentrated to afford the crude product, which was further purified by silica gel column chromatography to give the parent aldehyde/ketone.
References:
Du, Yunfei;Ouyang, Yaxin;Wang, Xi;Wang, Xiaofan;Yu, Zhenyang;Zhao, Bingyue;Zhao, Kang [Arkivoc,2021,vol. 2021,# 7,p. 48 - 65]
1703-46-4
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100-10-7
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6203-18-5
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100-10-7
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459-57-4
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124-40-3
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100-10-7
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$5.00/1g