4-ethoxy-N-methoxy-N-methylbenzamide synthesis
- Product Name:4-ethoxy-N-methoxy-N-methylbenzamide
- CAS Number:1221341-06-5
- Molecular formula:C11H15NO3
- Molecular Weight:209.24
619-86-3
244 suppliers
$15.00/25g
6638-79-5
590 suppliers
$6.00/25g
1221341-06-5
4 suppliers
inquiry
Yield:-
Reaction Conditions:
Stage #1: 4-(ethoxy)benzoic acidwith oxalyl dichloride;N,N-dimethyl-formamide in dichloromethane at 20; for 3 h;Inert atmosphere;
Stage #2: O,N-dimethyl-hydroxylamine hydrochloridewith triethylamine in dichloromethane at 0;Inert atmosphere;
References:
Komatsuda, Masaaki;Kondo, Hiroki;Ohki, Hugo;Suto, Ayane;Yamaguchi, Junichiro [Organic Letters,2022,vol. 24,# 17,p. 3270 - 3274] Location in patent:supporting information