4-HYDROXY-3-METHOXYCINNAMIDE synthesis
- Product Name:4-HYDROXY-3-METHOXYCINNAMIDE
- CAS Number:19272-90-3
- Molecular formula:C10H11NO3
- Molecular Weight:193.2
1135-24-6
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Yield:-
Steps:
Multi-step reaction with 4 steps
1: dmap / 0 - 10 °C
2: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 2 h / 0 °C
3: ammonium hydroxide; water / dichloromethane / 0 °C
4: sodium methylate; methanol / 0.25 h / 0 °C
References:
Badavath, Vishnu N.;Baysal, Ipek;Uar, Gülberk;Mondal, Susanta K.;Sinha, Barij N.;Jayaprakash, Venkatesan [Archiv der Pharmazie,2016,vol. 349,# 1,p. 9 - 19]
121-33-5
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19272-90-3
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