4-HYDROXY-6-METHOXYMETHYL-2-(METHYLTHIO)PYRIMIDINE synthesis
- Product Name:4-HYDROXY-6-METHOXYMETHYL-2-(METHYLTHIO)PYRIMIDINE
- CAS Number:68087-13-8
- Molecular formula:C7H10N2O2S
- Molecular Weight:186.23
68087-13-8
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Yield:-
Steps:
Multi-step reaction with 4 steps
1: N-chloro-succinimide / dichloromethane; N,N-dimethyl-formamide / 4 h / 20 °C
2: 2,6-dimethylpyridine / dichloromethane / 2 h / 0 - 20 °C
3: caesium carbonate / tetrakis(triphenylphosphine) palladium(0) / 1 h / 140 °C
4: boron tribromide / dichloromethane / 1 h / 0 °C
References:
WO2012/58187,2012,A1
68087-13-8
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1374134-65-2
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68087-13-8
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1374134-61-8
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