4-HYDROXY-7-IODOQUINOLINE synthesis
- Product Name:4-HYDROXY-7-IODOQUINOLINE
- CAS Number:22297-71-8
- Molecular formula:C9H6INO
- Molecular Weight:271.05
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Yield:22297-71-8 98%
Reaction Conditions:
at 280; for 15 h;
Steps:
6
Compound 6-E (5.5 g) was placed I a 100 mL round bottom flask and heated under N2 in an oil bath to 280 C for 15 minutes. 7-iodoquinolin-4-ol 6-F (4.6 g, 99% yield) was obtained as a solid.
References:
WO2005/63739,2005,A1 Location in patent:Page/Page column 53
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$8.00/5g
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