4-(MethoxyMethyl) cyclohexaneMethanol synthesis
- Product Name:4-(MethoxyMethyl) cyclohexaneMethanol
- CAS Number:98955-27-2
- Molecular formula:C9H18O2
- Molecular Weight:158.24
32529-79-6
89 suppliers
$6.00/250mg
13380-85-3
66 suppliers
$42.00/250mg
51181-40-9
23 suppliers
inquiry
98955-27-2
51 suppliers
$40.00/100mg
Yield:13380-85-3 80 %Chromat. ，98955-27-2 8 %Chromat. ，51181-40-9 7 %Chromat.
Reaction Conditions:
with hydrogen in lithium hydroxide monohydrate at 110; under 37503.8 Torr; for 18 h;Autoclave;
Steps:
5 Examples 2 to 5
General procedure: 1 mmol of the substrate as described in the table below, 100 mg of Catalyst (1) [Pt that is 2 mol % of the substrate, Mo that is 0.5 mol % of the substrate (in terms of metal)], and 3 mL of water were charged in an autoclave having a Teflon (trade name) inner cylinder and reacted at 110° C. for a number of hours as described in the table below under the condition of hydrogen pressure of 5 MPa to produce reaction products. The conversion ratio (conv. [%]) of the substrate was measured using HPLC, and the yield of each one of the reaction products was measured using a gas chromatograph mass spectrometer (GC-MS).
References:
US2022/127218,2022,A1 Location in patent:Paragraph 0104-0105
105-08-8
370 suppliers
$5.00/25g
98955-27-2
51 suppliers
$40.00/100mg
105-08-8
370 suppliers
$5.00/25g
74-88-4
349 suppliers
$15.00/10g
98955-27-2
51 suppliers
$40.00/100mg