4-O-Feruloylquinic acid synthesis
- Product Name:4-O-Feruloylquinic acid
- CAS Number:2613-86-7
- Molecular formula:C17H20O9
- Molecular Weight:368.34
77-95-2
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Yield:-
Steps:
Multi-step reaction with 4 steps
1.1: toluene-4-sulfonic acid / toluene; N,N-dimethyl-formamide / 18 h / Inert atmosphere; Dean-Stark; Reflux
2.1: dmap; tetra-(n-butyl)ammonium iodide; triethylamine / N,N-dimethyl-formamide / 6 h / -10 - 20 °C / Inert atmosphere
3.1: dmap; pyridine / 20 °C / Inert atmosphere
4.1: hydrogenchloride / tetrahydrofuran; water / 120 h / 20 °C / Inert atmosphere
4.2: Inert atmosphere; Heating
References:
Dokli, Irena;Navarini, Luciano;Hamersak, Zdenko [Tetrahedron Asymmetry,2013,vol. 24,# 13-14,p. 785 - 790]
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1135-24-6
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