4-TERT-BUTYL-2,6-DICHLOROPHENOL synthesis
- Product Name:4-TERT-BUTYL-2,6-DICHLOROPHENOL
- CAS Number:34593-75-4
- Molecular formula:C{10}H{12}Cl{2}O
- Molecular Weight:0
96-76-4
394 suppliers
$6.00/25g
98-28-2
69 suppliers
$49.00/100g
34593-75-4
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4166-86-3
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Yield:4166-86-3 70% ，98-28-2 16% ，34593-75-4 14%
Reaction Conditions:
with copper chloride (II) in acetonitrile at 80; for 6 h;Overall yield = 100 percent;
Steps:
11.2-11.3
2) 2.0mmol 2,4-di-tert-butylphenol, 2.0mmol CuCl2, 2.0mol% titanium-aluminum binary oxide catalyst was dissolved in 10mL CH3CN, stir at 80°C for 6h;3) The reaction mixture is filtered and extracted.The filtrate was diluted with distilled water and transferred to a separatory funnel.The resulting mixture was used with CH2Cl2(3 × 15 mL), the organic layer was extracted with Na2CO3The solution (1.0 mol L-1) was washed continuously until no bubbles were formed.CH2Cl2layer over anhydrous Na2SO4After drying, filtration, and concentration, it is used for further identification and quantitative testing.
References:
CN114057550,2022,A Location in patent:Paragraph 0100; 0102-0103; 0131-0132
96-76-4
394 suppliers
$6.00/25g
98-54-4
425 suppliers
$16.00/25g
98-28-2
69 suppliers
$49.00/100g
34593-75-4
9 suppliers
inquiry
4166-86-3
6 suppliers
inquiry
34896-06-5
0 suppliers
inquiry
34593-75-4
9 suppliers
inquiry
98-54-4
425 suppliers
$16.00/25g
34593-75-4
9 suppliers
inquiry