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ChemicalBook CAS DataBase List 5,7-Dihydroxy-6,8-dimethylchromone
21722-27-0

5,7-Dihydroxy-6,8-dimethylchromone synthesis

2synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 3 steps
1.1: boron trifluoride diethyl etherate / 1.5 h / 0 - 90 °C / Inert atmosphere
2.1: sodium hydride / mineral oil / 2.83 h / 0 °C / Inert atmosphere
2.2: 0 - 20 °C
3.1: aluminum (III) chloride / benzene / 3 h / 90 °C / Inert atmosphere
3.2: 2 h / 0 °C

References:

Katagiri, Ryo;Kiuchi, Fumiyuki;Narukawa, Yuji;Uekusa, Yoshinori [Heterocycles,2020,vol. 100,# 5,p. 803 - 808]

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