5-BROMO-2-(4-METHOXYPHENOXY)PYRIMIDINE synthesis
- Product Name:5-BROMO-2-(4-METHOXYPHENOXY)PYRIMIDINE
- CAS Number:69033-87-0
- Molecular formula:C11H9BrN2O2
- Molecular Weight:281.11
38353-06-9
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$15.00/1g
150-76-5
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69033-87-0
28 suppliers
$238.00/1g
Yield:69033-87-0 71%
Reaction Conditions:
Stage #1: 5-bromo-1H-pyrimidin-2-onewith (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate;caesium carbonate in tetrahydrofuran at 20; for 0.833333 h;Inert atmosphere;
Stage #2: 4-methoxy-phenolwith caesium carbonate in tetrahydrofuran at 20; for 0.75 h;
References:
Kokatla, Hari Prasad;Lakshman, Mahesh K. [Organic Letters,2010,vol. 12,# 20,p. 4478 - 4481] Location in patent:supporting information; experimental part
150-76-5
820 suppliers
$5.00/5G
32779-36-5
633 suppliers
$5.00/5g
69033-87-0
28 suppliers
$238.00/1g