5-BROMO-4-PYRIMIDINECARBOXALDEHYDE synthesis
- Product Name:5-BROMO-4-PYRIMIDINECARBOXALDEHYDE
- CAS Number:933746-26-0
- Molecular formula:C5H3BrN2O
- Molecular Weight:186.99
64224-60-8
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Yield:-
Steps:
Multi-step reaction with 2 steps
1.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 20 °C / Inert atmosphere
1.2: 1 h / 0 °C / Inert atmosphere
2.1: diisobutylaluminium hydride / tetrahydrofuran / 1 h / -10 °C / Inert atmosphere
References:
WO2016/59412,2016,A1