ChemicalBook CAS DataBase List 5-Fluoro-2-methylindole

5-Fluoro-2-methylindole synthesis

12synthesis methods

Product Name:5-Fluoro-2-methylindole
CAS Number:399-72-4
Molecular formula:C9H8FN
Molecular Weight:149.16

1-(5-fluoro-2-nitrophenyl) propane-2-one (0.5mmol, 99 mg), zinc powder (3.0mmol, 196 mg), and acetic acid (6.0mmol, 360 mg) was added to the reaction tube, followed by adding ethanol to 2 ml at 90 °C for 3h. After cooling to room temperature, the reaction system was added 20 ml water. 5-Fluoro-2-methylindole was obtained after purification.

823-85-8 Synthesis

823-85-8
372 suppliers
$5.00/5g

399-72-4
243 suppliers
$10.00/1g

Yield:-

Steps:

Multi-step reaction with 2 steps
1: aq. NaHCO₃ / CH₂Cl₂ / 3 h / 20 °C
2: ZnCl₂ / 140 °C

References:

McKew, John C.;Foley, Megan A.;Thakker, Paresh;Behnke, Mark L.;Lovering, Frank E.;Sum, Fuk-Wah;Tam, Steve;Wu, Kun;Shen, Marina W. H.;Zhang, Wen;Gonzalez, Mario;Liu, Shanghao;Mahadevan, Anu;Sard, Howard;Khor, Soo Peang;Clark, James D. [Journal of Medicinal Chemistry,2006,vol. 49,# 1,p. 135 - 158]

1266659-06-6 Synthesis

1266659-06-6
17 suppliers
$972.00/5g

399-72-4
243 suppliers
$10.00/1g

References

557-93-7
231 suppliers
$45.10/5g

1003-98-1 Synthesis

1003-98-1
408 suppliers
$5.00/5g

399-72-4
243 suppliers
$10.00/1g

References

399-52-0 Synthesis

399-52-0
391 suppliers
$10.00/1g

74-88-4
349 suppliers
$15.00/10g

399-72-4
243 suppliers
$10.00/1g

References

371-14-2 Synthesis

371-14-2
88 suppliers
inquiry

399-72-4
243 suppliers
$10.00/1g

815586-68-6
50 suppliers
$78.00/0.25 / G

References

5-Fluoro-2-methylindole Related Search:

2-Methylindole 3-Methylindole Indole Fluorine 5-Fluoroindole-2-carboxylic acid 5-Fluoroindole 4-Fluoroindole 5-Fluoro-3-methylindole (5-FLUORO-1H-INDOL-2-YL)METHANAMINE 8-FLUORO-2,3,4,5-TETRAHYDRO-1H-PYRIDO[4,3-B]INDOLE

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5-Fluoro-2-methylindole synthesis

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