5-PHENYL-O-ANISIDINE synthesis
- Product Name:5-PHENYL-O-ANISIDINE
- CAS Number:39811-17-1
- Molecular formula:C13H13NO
- Molecular Weight:199.25
15854-73-6
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Yield: 99%
Reaction Conditions:
with palladium 10% on activated carbon;hydrogen in methanol for 8 h;
Steps:
1
Compound II-3 (669 mg, 2.91 mmol)Soluble in methanol (9.7mL, 0.3M),Add 10% Pd/C (67 mg),After reacting for 8 hours under hydrogen pressure,TLC monitoring showed the end of the reaction.Diatomaceous earth suction filtration,The filtrate was dried under reduced pressure to give compound II-4(Brown solid, 575 mg, yield 99%).
References:
China Pharmaceutical University;Yan Dingfei;Cheng Yalong;Sun Hongbin CN109293537, 2019, A Location in patent:Paragraph 0044; 0046; 0049
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