C-(3-CHLORO-PHENYL)-C-PHENYL-METHYLAMINE HYDROCHLORIDE synthesis

2synthesis methods

Product Name:C-(3-CHLORO-PHENYL)-C-PHENYL-METHYLAMINE HYDROCHLORIDE
CAS Number:5267-37-8
Molecular formula:C13H12ClN.ClH
Molecular Weight:254.159

3-chlorobenzophenone (43.33g, 0.2 mol) and ammonium formate (63.06g, 1.0 mol) were refluxed for 3 hours in nitrobenzene (250 ml). After cooling the refluxed mixture to room temperature, the reaction solution was concentrated in vacuo. The 15% HCl-ethanol solution (420 ml) was added to the residue, and the mixture was refluxed for 2 hours. Then the reaction solution was concentrated in vacuo. Thereafter, the diethyl ether was added. Finally, C-(3-CHLORO-PHENYL)-C-PHENYL-METHYLAMINE HYDROCHLORIDE was obtained by filtration.

C-(3-CHLORO-PHENYL)-C-PHENYL-METHYLAMINE HYDROCHLORIDE

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Yield:-

Steps:

Multi-step reaction with 2 steps
1: 69 percent / NH₂OH*HCl; Na₂CO₃ / ethanol / 15 h / Heating
2: 45 percent / NaBH₄; TiCl₄ / 1,2-dimethoxy-ethane / 24 h / 20 °C

References:

Sasse;Stark;Ligneau;Elz;Reidemeister;Ganellin;Schwartz;Schunack [Bioorganic and Medicinal Chemistry,2000,vol. 8,# 5,p. 1139 - 1149]

Ethanamine, N-[(3,5-dichlorophenyl)methylene]-2,2-diethoxy-

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References

C-(3-CHLORO-PHENYL)-C-PHENYL-METHYLAMINE HYDROCHLORIDE Related Search:

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C-(3-CHLORO-PHENYL)-C-PHENYL-METHYLAMINE HYDROCHLORIDE synthesis

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