1-[(Phenylmethoxy)carbonyl]-L-prolyl-β-alanine Methyl Ester synthesis
- Product Name:1-[(Phenylmethoxy)carbonyl]-L-prolyl-β-alanine Methyl Ester
- CAS Number:59543-05-4
- Molecular formula:C17H22N2O5
- Molecular Weight:334.37
Yield:59543-05-4 100%
Reaction Conditions:
Stage #1: N-Benzyloxycarbonyl-L-prolinewith 4-methyl-morpholine;isobutyl chloroformate in tetrahydrofuran at -25; for 0.166667 h;
Stage #2: methyl 3-aminopropanoate hydrochloridewith 4-methyl-morpholine in tetrahydrofuran at -25; for 2 h;
References:
Erkkil?, Anniina;Pihko, Petri M. [Journal of Organic Chemistry,2006,vol. 71,# 6,p. 2538 - 2541]
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