6-Methoxyquinoline synthesis
- Product Name:6-Methoxyquinoline
- CAS Number:5263-87-6
- Molecular formula:C10H9NO
- Molecular Weight:159.18
Yield:5263-87-6 72%
Reaction Conditions:
with transition metal catalyst;pyridine derviative;acid derviative at 150; for 12 h;Green chemistry;
Steps:
25
Accurately weigh 0.005mmol (l. Lmg) of the transition metal, add 10mL has been put into the magnetic stirrer Young's reaction tube, The oxygen reaction was carried out in the Young's reaction tube, and the reaction was carried out under oxygen conditions. The syringe was applied to the Young's reaction tube0.04 mmol of co-catalyst I, 0.08 mmol of co-catalyst II, 0.2 mmol of 4-methoxyaniline and 1 ml of 1,3-Propylene glycol, the Young's reaction tube was placed on a magnetic stirrer and stirred at 150 ° C for 12 h. After completion of the reaction, the reaction solutionThe pH of the neutral, the reaction solution for post-processing, 6-methoxyquinoline pure product, the yield of 72%.
References:
Suzhou Research Institute, Lanzhou Institute of Chemical Physics (LICP) of the Chinese Academy of Sciences (CAS);Jiang, Gaoxi;Li, Jixing;Yang, Huimeng;Xia, Chungu CN106543078, 2017, A Location in patent:Paragraph 0107; 0108
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