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ChemicalBook CAS DataBase List Ethyl2-(4-Bromophenyl)-4-methylthiazole-5-carboxylate
61291-89-2

Ethyl2-(4-Bromophenyl)-4-methylthiazole-5-carboxylate synthesis

2synthesis methods
-

Yield:61291-89-2 73%

Reaction Conditions:

in ethanol; for 5 h;Inert atmosphere;Reflux;

Steps:

2.3.2. General procedure for the synthesis of compounds3a-3e from compounds 2a-2e

General procedure: The synthetic procedure of compounds 3a-3e: To a stirredsolution of 2a-2e (20 mmol) in EtOH (40 mL) and was addedethyl 2-chloro-3-oxobutanoate (20 mmol, 3.29 g), the reactionmixture was heated at reflux in N2 atmosphere until the completion of reaction as indicated by TLC analysis (typicallywithin 5 h).The reaction mixture was poured into ice-water (100 mL)and the mixture thus obtained was extracted with CH2Cl2(100 mL 3). The combined organic phases were washedwith saturated brine (300 mL), dried over anhydrous Na2SO4and evaporated on a rotary evaporator to afford a residue,which was purified by column chromatography through ashort silica gel column to yield 3a-3e.

References:

Wu, Jingwei;Li, Weiya;Zheng, Zhihui;Lu, Xinhua;Zhang, Huan;Ma, Ying;Wang, Runling [Journal of Biomolecular Structure and Dynamics,2021,vol. 39,# 4,p. 1174 - 1188]

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