N-(3-methoxyphenyl)-2-morpholin-4-yl-2-oxo-acetamide synthesis
- Product Name:N-(3-methoxyphenyl)-2-morpholin-4-yl-2-oxo-acetamide
- CAS Number:6608-47-5
- Molecular formula:C2H3ClO2S
- Molecular Weight:126.56
31469-08-6
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6608-47-5
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Yield:6608-47-5 92%
Reaction Conditions:
with triethylamine in dichloromethane at 20;stereospecific reaction;
Steps:
6. General experimental procedure for (E)-conjugated polyene sulfonyl chloride
General procedure: 1 mmol compound 2 was dissolve in 10~20 mL DCM. 2 equiv TEA was added dropwise at room temperature. Stirred for several minutes, the reaction mixture was washed with brine (5~10 mL). The organic layer was dried over anhydrous Na2SO4, filtered and concentrated to yield faintly yellow or colorless oil product with 85-95% yield.
References:
Yu, Chunyan;Lv, Zhongwen;Xu, Sheng;Zhang, Jun [Tetrahedron Letters,2018,vol. 59,# 34,p. 3234 - 3237] Location in patent:supporting information
1622-32-8
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6608-47-5
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1184-84-5
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6608-47-5
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3039-83-6
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6608-47-5
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15805-34-2
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6608-47-5
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