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ChemicalBook CAS DataBase List [[[(2R,3S,4R,5R)-5-(2-amino-6-oxo-3H-purin-9-yl)-3,4-dihydroxyoxolan-2-yl]methoxy-hydroxyphosphoryl]oxy-hydroxyphosphoryl] [(2R,3S,4R,5R)-5-(2-amino-6-oxo-3H-purin-9-yl)-3,4-dihydroxyoxolan-2-yl]methyl hydrogen phosphate
6674-45-9

[[[(2R,3S,4R,5R)-5-(2-amino-6-oxo-3H-purin-9-yl)-3,4-dihydroxyoxolan-2-yl]methoxy-hydroxyphosphoryl]oxy-hydroxyphosphoryl] [(2R,3S,4R,5R)-5-(2-amino-6-oxo-3H-purin-9-yl)-3,4-dihydroxyoxolan-2-yl]methyl hydrogen phosphate synthesis

1synthesis methods
-

Yield:6674-45-9 71%

Reaction Conditions:

with pyridine;1-methyl-pyrrolidin-2-one;N,N,N,N,N,N-hexamethylphosphoric triamide;tributyl-amine;S,S'-bis(4-chlorophenyl) phosphorodithioate;silver nitrate at 0 - 20; for 7 h;

References:

Fukuoka, Koichiro;Suda, Fuminori;Suzuki, Ryo;Ishikawa, Masahide;Hata, Tsujiaki [Chemistry Letters,1994,# 3,p. 499 - 502]

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