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ChemicalBook CAS DataBase List TERT-BUTYL 4-(2-AMINOPHENOXY)TETRAHYDRO-1(2H)-PYRIDINECARBOXYLATE
690632-14-5

TERT-BUTYL 4-(2-AMINOPHENOXY)TETRAHYDRO-1(2H)-PYRIDINECARBOXYLATE synthesis

3synthesis methods
-

Yield:690632-14-5 432 mg

Reaction Conditions:

Stage #1: tert-butyl 4-(2-nitrophenoxy)piperidine-1-carboxylate in methanol;Inert atmosphere;
Stage #2: with 20% Pd/C;hydrogen in methanol at 20;

Steps:

General procedure B.

General procedure: Nitro compound (1 eq.) was dissolved in MeOH (20mL/mmol) and the mixture was stirred for 30min under argon atmosphere after which Pd/C (20m/m%) was added and the reaction mixture was stirred under hydrogen atmosphere for 2h. The catalyst was filtered off and the solvent removed under reduced pressure to obtain the product.

References:

Skok, ?iga;Durcik, Martina;Zajec, ?iva;Gramec Skledar, Darja;Bozovi?ar, Kri?tof;Pi?lar, Anja;Toma?i?, Tihomir;Zega, Anamarija;Peterlin Ma?i?, Lucija;Kikelj, Danijel;Zidar, Nace;Ila?, Janez [European Journal of Medicinal Chemistry,2023,vol. 249,art. no. 115116]

TERT-BUTYL 4-(2-AMINOPHENOXY)TETRAHYDRO-1(2H)-PYRIDINECARBOXYLATE Related Search:

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