7-Iodo Sancycline synthesis
- Product Name:7-Iodo Sancycline
- CAS Number:113164-67-3
- Molecular formula:C21H21IN2O7
- Molecular Weight:540.31
64-73-3
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Yield:-
Steps:
Multi-step reaction with 3 steps
1: triethylamine; palladium on activated charcoal; hydrogen / ethanol
2: rhodium contaminated with carbon; hydrogen; toluene-4-sulfonic acid / methanol / -5 - 5 °C
3: sulfuric acid; N-iodo-succinimide / 2 h / 0 - 10 °C
References:
CN106831479,2017,A
987-02-0
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113164-67-3
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