ChemicalBook CAS DataBase List 7-Methoxy-1H-indole

7-Methoxy-1H-indole synthesis

10synthesis methods

Product Name:7-Methoxy-1H-indole
CAS Number:3189-22-8
Molecular formula:C9H9NO
Molecular Weight:147.17

2486-69-3 Synthesis

2486-69-3
251 suppliers
$8.00/1g

3189-22-8
267 suppliers
$16.00/1g

Yield:-

Steps:

Multi-step reaction with 6 steps
1: SOCl₂ / 2 h / 20 °C
2: 99 percent / bis(pyridine)iodonium(I) tetrafluoroborate; CF₃SO₃H / CH₂Cl₂ / 16 h / 20 °C
3: 90 percent / Et₃N / Pd(PPh₃)2Cl₂-CuI / 3 h / 0 - 20 °C
4: 69 percent / CuI / dimethylformamide / 2.5 h / 100 °C
5: 95 percent / KOH; H₂O / ethanol / 24 h / Heating
6: 65 percent / Cu₂O / quinoline / 4 h / 230 °C

References:

Ezquerra, Jesus;Pedregal, Concepcion;Lamas, Carlos;Barluenga, Jose;Perez, Marta;Garcia-Martin, Miguel Angel;Gonzalez, Jose M. [Journal of Organic Chemistry,1996,vol. 61,# 17,p. 5804 - 5812]

1-(2-(3-METHOXY-2-NITRO-PHENYL)-VINYL)-PYRROLIDINE

96096-68-3
5 suppliers
$57.00/50mg

3189-22-8
267 suppliers
$16.00/1g

References

2-(5-chloro-3-methoxy-2-nitrophenyl)acetonitrile

111795-91-6
2 suppliers
inquiry

3189-22-8
267 suppliers
$16.00/1g

References

180623-99-8
8 suppliers
inquiry

3189-22-8
267 suppliers
$16.00/1g

References

5345-42-6
190 suppliers
$13.30/1g

3189-22-8
267 suppliers
$16.00/1g

References

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7-Methoxy-1H-indole synthesis

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