(5Z)-4-Chloro-N-(4-methoxyphenyl)-5H-1,2,3-dithiazol-5-imine synthesis
- Product Name:(5Z)-4-Chloro-N-(4-methoxyphenyl)-5H-1,2,3-dithiazol-5-imine
- CAS Number:75318-49-9
- Molecular formula:C9H7ClN2OS2
- Molecular Weight:258.75
Yield:75318-49-9 99%
Reaction Conditions:
Stage #1: 4-methoxy-aniline;4,5-dichloro-1,2,3-dithiazolium chloride in dichloromethane at 20; for 1 h;Inert atmosphere;
Stage #2: with pyridine in dichloromethane at 20;Inert atmosphere;
References:
McCutcheon, David C.;Paley, Miranda A.;Steinhardt, Rachel C.;Prescher, Jennifer A. [Journal of the American Chemical Society,2012,vol. 134,# 18,p. 7604 - 7607] Location in patent:supporting information; experimental part
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