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ChemicalBook CAS DataBase List BZ-DMT-DEOXYADENOSINE 2-CLPH DIESTER TRIETHYLAMMONIUM SALT
85381-22-2

BZ-DMT-DEOXYADENOSINE 2-CLPH DIESTER TRIETHYLAMMONIUM SALT synthesis

1synthesis methods
64325-78-6 Synthesis
N6-Benzoyl-5'-O-(4,4'-dimethoxytrityl)-2'-deoxyadenosine

64325-78-6
190 suppliers
$9.00/250mg

15074-54-1 Synthesis
2-CHLOROPHENYL PHOSPHORODICHLORIDATE

15074-54-1
86 suppliers
$19.00/1g

-

Yield:-

Reaction Conditions:

Stage #1: N6-benzoyl-5'-O-(4,4'-dimethoxytrityl)-2'-deoxyadenosine;2-chlorophenyl dichlorophosphatewith pyridine;1,2,3-triazole in dichloromethane at 0; for 2.5 h;
Stage #2: triethylamine carbonatewith water in dichloromethane;Further stages.;

References:

Yagodkin, Andrey;Azhayev, Alex;Roivainen, Jarkko;Antopolsky, Maxim;Kayushin, Alexei;Korosteleva, Maria;Miroshnikov, Anatoly;Randolph, John;Mackie, Hugh [Nucleosides, nucleotides and nucleic acids,2007,vol. 26,# 5,p. 473 - 497]

BZ-DMT-DEOXYADENOSINE 2-CLPH DIESTER TRIETHYLAMMONIUM SALT Related Search:

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