Acetic acid, 2-[(1-chloro-2,2,2-trifluoroethyl)thio]-, methyl ester synthesis
1synthesis methods
- Product Name:Acetic acid, 2-[(1-chloro-2,2,2-trifluoroethyl)thio]-, methyl ester
- CAS Number:885460-98-0
- Molecular formula:C5H6ClF3O2S
- Molecular Weight:222.61
Yield:885460-98-0 63%
Reaction Conditions:
with sodium dithionite;sodium hydrogencarbonate in dimethyl sulfoxide at 35 - 45;
References:
Pustovit, Yuriy;Alexeenko, Anatoliy;Trofymchuk, Sergii;Lukin, Oleg;Tolmachev, Andrey A. [Synthesis,2010,# 7,art. no. T18809SS,p. 1159 - 1165] Location in patent:experimental part