ethyl 5-oxo-5,6,7,8-tetrahydronaphthalene-2-carboxylate synthesis
- Product Name:ethyl 5-oxo-5,6,7,8-tetrahydronaphthalene-2-carboxylate
- CAS Number:90401-85-7
- Molecular formula:C13H14O3
- Molecular Weight:218.25
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Yield:-
Steps:
Multi-step reaction with 3 steps
1: 62 percent / NaNO2, CuSO4 / H2O; aq. HCl / 2 h / 0 °C
2: 38 percent / KOH / ethanol; H2O / 4 h / Heating
3: 62 percent / HCl (20percent) / 3 h / Heating
References:
Itoh;Miyake;Tada;Hirata;Oka [Chemical and Pharmaceutical Bulletin,1984,vol. 32,# 1,p. 130 - 151]
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