5-(4,4,5,5-TETRAMETHYL-[1,3,2]DIOXABOROLAN-2-YL)-PYRIDINE-2-CARBOXYLIC ACID DIETHYLAMIDE synthesis

4synthesis methods

Product Name:5-(4,4,5,5-TETRAMETHYL-[1,3,2]DIOXABOROLAN-2-YL)-PYRIDINE-2-CARBOXYLIC ACID DIETHYLAMIDE
CAS Number:911227-46-8
Molecular formula:C16H25BN2O3
Molecular Weight:304.19

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73183-34-3
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5-(4,4,5,5-TETRAMETHYL-[1,3,2]DIOXABOROLAN-2-YL)-PYRIDINE-2-CARBOXYLIC ACID DIETHYLAMIDE

911227-46-8
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$254.00/500mg

Yield:911227-46-8 74%

Reaction Conditions:

Stage #1: bis(pinacol)diboranewith (1,5-cyclooctadiene)(methoxy)iridium(I) dimer;4,4'-bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-2,2’-bipyridine in hexane at 60; for 0.5 h;Inert atmosphere;Glovebox;Sealed tube;
Stage #2: N,N-diethyl-2-pyridinecarboxamidewith bis(2,6-di-tert-butyl-4-methylphenoxide)methylaluminum in hexane at 20; for 18 h;Sealed tube;

References:

Yang, Lichen;Semba, Kazuhiko;Nakao, Yoshiaki [Angewandte Chemie - International Edition,2017,vol. 56,# 17,p. 4853 - 4857][Angew. Chem.,2017,vol. 129,# 17,p. 4931 - 4935] Location in patent:supporting information

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673485-54-6 Synthesis

5-BROMO-PYRIDINE-2-CARBOXYLIC ACID DIETHYLAMIDE

673485-54-6
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911227-46-8
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References

673485-54-6 Synthesis

673485-54-6
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911227-46-8
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References

137178-88-2
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911227-46-8
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References

5-(4,4,5,5-TETRAMETHYL-[1,3,2]DIOXABOROLAN-2-YL)-PYRIDINE-2-CARBOXYLIC ACID DIETHYLAMIDE Related Search:

2-(CYCLOPROPYLMETHOXY)-5-(4,4,5,5-TETRAMETHYL-1,3,2-DIOXABOROLAN-2-YL)PYRIDINE 4-[5-(4,4,5,5-TETRAMETHYL-[1,3,2]DIOXABOROLAN-2-YL)-PYRIDIN-2-YL]-PIPERAZINE-1-CARBOXYLIC ACID TERT-BUTYL ESTER TERT-BUTYL N-METHYL-N-[5-(4,4,5,5-TETRAMETHYL-[1,3,2]DIOXABOROLAN-2-YL)PYRIDIN-2-YL]CARBAMATE 6-(4-FLUOROPHENYL)PYRIDINE-3-BORONIC ACID PINACOL ESTER 1-METHYL-4-[5-(4,4,5,5-TETRAMETHYL-1,3,2-DIOXABORALAN-2-YL)PYRIDINE-2-YL]PIPERAZINE Methyl 5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)picolinate 2-METHYLSULFANYL-5-(4,4,5,5-TETRAMETHYL-[1,3,2]-DIOXABOROLAN-2-YL)PYRIDINE 2-FORMYLPYRIDINE-5-BORONIC ACID PINACOLATE 2-(N-Methylaminocarbonyl)-5-pyridineboronic acid pincol ester

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5-(4,4,5,5-TETRAMETHYL-[1,3,2]DIOXABOROLAN-2-YL)-PYRIDINE-2-CARBOXYLIC ACID DIETHYLAMIDE synthesis

5-(4,4,5,5-TETRAMETHYL-[1,3,2]DIOXABOROLAN-2-YL)-PYRIDINE-2-CARBOXYLIC ACID DIETHYLAMIDE Related Search: