AC-GLU-NH2 synthesis
- Product Name:AC-GLU-NH2
- CAS Number:25460-87-1
- Molecular formula:C7H12N2O4
- Molecular Weight:188.18
108-24-7
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133464-46-7
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25460-87-1
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Yield:-
Reaction Conditions:
Stage #1: (S)-2-[((9H-fluoren-9-yl)methoxy)carbonylamino]-5-(allyloxy)-5-oxopentanoic acidwith N-ethyl-N,N-diisopropylamine;N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate in N,N-dimethyl-formamide; under 760.051 Torr; for 2 h;Inert atmosphere;Schlenk technique;
Stage #2: with 4-methylpiperidin in N,N-dimethyl-formamide;Inert atmosphere;Schlenk technique;
Stage #3: acetic anhydrideFurther stages;
References:
Jun, Joomyung V.;Raines, Ronald T. [Organic Letters,2021,vol. 23,# 8,p. 3110 - 3114] Location in patent:supporting information
636-65-7
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830-03-5
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25460-87-1
42 suppliers
$401.00/250mg