ChemicalBook CAS DataBase List ACIVICIN

ACIVICIN synthesis

11synthesis methods

Product Name:ACIVICIN
CAS Number:42228-92-2
Molecular formula:C5H7ClN2O3
Molecular Weight:178.57

56-86-0 Synthesis

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Yield:-

Steps:

Multi-step reaction with 9 steps
1: Cl₂, H₂SO₄ / 5 h / Irradiation
2: 85 percent / pH 9
3: 85 percent / dicyclohexylcarbodiimide / ethyl acetate / 0 °C
4: tetrahydrofuran / -50 - -30 °C
5: hydroxylamine / H₂O / pH 6
6: Et₃N / H₂O / Ambient temperature; pH 11
7: tetrahydrofuran
8: 54 percent / dichlorotris(dimethylamino)phosphorane / tetrahydrofuran / Heating
9: 87 percent / trifluoroacetic acid, thioanisole

References:

Silverman, Richard B.;Holladay, Mark W. [Journal of the American Chemical Society,1981,vol. 103,# 24,p. 7357 - 7358]

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References

Ethanamine, N-[(3,5-dichlorophenyl)methylene]-2,2-diethoxy-

1000210-73-0
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42228-92-2
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References

1000210-73-0
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42228-92-2
93 suppliers
$40.00/1mg

References

1000210-73-0
0 suppliers
inquiry

42228-92-2
93 suppliers
$40.00/1mg

References

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ACIVICIN synthesis

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