Allylmagnesium chloride synthesis
- Product Name:Allylmagnesium chloride
- CAS Number:2622-05-1
- Molecular formula:C3H5ClMg
- Molecular Weight:100.83
75-54-7
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107-05-1
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$16.80/100ML
2622-05-1
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$40.00/500mg
Yield:-
Reaction Conditions:
with magnesium in tetrahydrofuran
Steps:
R.5 Synthesis of diallylmethylchlorosilane
REFERENCE EXAMPLE 5 Synthesis of diallylmethylchlorosilane Allylmagnesium chloride was synthesised by the gradual dropwise addition of 50 parts of allyl chloride to a mixture of 15 parts of magnesium turnings and 100 parts of tetrahydrofuran. This was gradually added dropwise over a period of 2 hours to 18 parts of methyldichlorosilane dissolved in 100 parts of tetrahydrofuran, and the reaction was then heated for an additional 1 hour under reflux.
References:
Dow Corning Asia, Ltd. US5502229, 1996, A
107-05-1
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2622-05-1
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$40.00/500mg
7439-95-4
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2622-05-1
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187737-37-7
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592-42-7
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613-12-7
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$203.00/1g
2622-05-1
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