ALPHA-D-MAN-[1->4]-ALPHA-D-MAN-1->OME synthesis
- Product Name:ALPHA-D-MAN-[1->4]-ALPHA-D-MAN-1->OME
- CAS Number:70427-91-7
- Molecular formula:C13H24O11
- Molecular Weight:356.32
65530-26-9
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Yield:-
Steps:
Multi-step reaction with 5 steps
1: 85 percent / sodium hydride / dimethylformamide / 20 h / 0 deg C to R.T.
2: 76 percent / sodium cyanoborohydride, 3A molecular sieves / tetrahydrofuran / 0.5 h / 0 °C
3: mercuric bromide, mercuric cyanide, 4A molecular sieves / acetonitrile / Ambient temperature; 6h then overnight
4: M sodium methoxide / methanol / 2 h / Ambient temperature
5: 91 percent / hydrogen / 10percent palladium-on-charcoal / aq. ethanol; acetic acid / 2625.2 Torr
References:
Madiyalakan, Ragupathy;Chowdhary, Manjit S.;Rana, Surjit S.;Matta, Khushi L. [Carbohydrate Research,1986,vol. 152,p. 183 - 194]
51842-18-3
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70427-91-7
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16697-49-7
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