ChemicalBook CAS DataBase List Atractylodin

Atractylodin synthesis

5synthesis methods

Product Name:Atractylodin
CAS Number:55290-63-6
Molecular formula:C13H10O
Molecular Weight:182.22

Ethanamine, N-[(3,5-dichlorophenyl)methylene]-2,2-diethoxy-

1000210-73-0
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55290-63-6
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Yield:-

Steps:

Multi-step reaction with 4 steps
1.1: n-BuLi / tetrahydrofuran; hexane / 2 h / -78 - 20 °C
1.2: 54 percent / tetrahydrofuran; hexane / -78 - 20 °C
2.1: 59 percent / manganese dioxide / CH₂Cl₂ / 20 °C
3.1: 58 percent / PPh₃ / CH₂Cl₂ / 20 °C
4.1: 72 percent / n-BuLi / hexane / 0.5 h / -78 - -40 °C

References:

Shi Shun, Annabelle L. K.;Tykwinski, Rik R. [Journal of Organic Chemistry,2003,vol. 68,# 17,p. 6810 - 6813]

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Silane, (5E)-5-heptene-1,3-diyn-1-yltrimethyl-

811861-64-0
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55290-63-6
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References

1000210-73-0
0 suppliers
inquiry

55290-63-6
216 suppliers
$49.00/5mg

References

1000210-73-0
0 suppliers
inquiry

55290-63-6
216 suppliers
$49.00/5mg

References

1000210-73-0
0 suppliers
inquiry

55290-63-6
216 suppliers
$49.00/5mg

References

Atractylodin Related Search:

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Atractylodin synthesis

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