BENZO(C)ACRIDINE synthesis
- Product Name:BENZO(C)ACRIDINE
- CAS Number:225-51-4
- Molecular formula:C17H11N
- Molecular Weight:229.28
66-99-9
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Yield:-
Steps:
Multi-step reaction with 4 steps
1.1: isopropylmagnesium chloride / tetrahydrofuran / 0.5 h / -40 - -20 °C / Inert atmosphere
1.2: -20 - 20 °C / Inert atmosphere
2.1: iodine; acetic acid; hypophosphorous acid / water / 60 °C
3.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 1 h / 0 - 20 °C
4.1: triphenylphosphine; sodium azide / N,N-dimethyl acetamide; water / 0.5 h / 120 °C / Inert atmosphere; Schlenk technique
4.2: 48 h / 120 °C / Inert atmosphere; Schlenk technique
References:
Wang, Ming;Fan, Qiaoling;Jiang, Xuefeng [Organic Letters,2018,vol. 20,# 1,p. 216 - 219]
![Ethanamine, N-[(3,5-dichlorophenyl)methylene]-2,2-diethoxy-](/CAS/20210305/GIF/1000210-73-0.gif)
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134-32-7
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6630-33-7
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225-51-4
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1000210-73-0
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