(-)-Benzotetramisole synthesis
- Product Name:(-)-Benzotetramisole
- CAS Number:950194-37-3
- Molecular formula:C15H12N2S
- Molecular Weight:252.33
615-20-3
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950194-37-3
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Yield:-
Steps:
Multi-step reaction with 2 steps
1.1: N-ethyl-N,N-diisopropylamine / 48 h / 135 °C / Inert atmosphere
2.1: methanesulfonyl chloride; triethylamine / dichloromethane / 2 h / 0 °C / Inert atmosphere
2.2: 0.5 h / 20 °C / Inert atmosphere
2.3: 12 h / 55 °C / Inert atmosphere
References:
Matsumoto, Takuya;Urano, Yasuteru;Takahashi, Yoshinori;Mori, Yusuke;Terai, Takuya;Nagano, Tetsuo [Journal of Organic Chemistry,2011,vol. 76,# 10,p. 3616 - 3625]
1235891-51-6
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950194-37-3
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