Benzyl carbamate synthesis
- Product Name:Benzyl carbamate
- CAS Number:621-84-1
- Molecular formula:C8H9NO2
- Molecular Weight:151.16
Yield:621-84-1 99%
Reaction Conditions:
with alumina supported nickel oxide-bismuth oxide oxide catalyst at 110; for 10 h;Sealed tube;
Steps:
4.B B. Preparation of benzyl carbamate
540g of urea, 3000mL of benzyl alcohol and 5.4 catalyst C were introduced into a 10L reaction kettle in sequence, sealed, heated to 110°C and reacted at this temperature for 10 hours to obtain benzyl carbamate.After testing, the yield of benzyl carbamate was 99.00%, and no benzyl carbamate was detected in the benzyl carbamate (exceeding the detection limit of 0.00001%).
References:
Chongqing Chemical Profession College;Ma Yubo;Luo Litong;Song Chunyu;Jiang Rongguang CN111662215, 2020, A Location in patent:Paragraph 0055; 0059-0061
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