Benzyl-PEG7-amino synthesis
- Product Name:Benzyl-PEG7-amino
- CAS Number:868594-43-8
- Molecular formula:C21H37NO7
- Molecular Weight:415.52
868594-42-7
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868594-43-8
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Yield:868594-43-8 97%
Reaction Conditions:
Stage #1: 1-azido-20-(phenylmethyloxy)-3,6,9,12,15,18-hexaoxaeicosanewith triphenylphosphine in tetrahydrofuran at 20; for 3 h;Staudinger reaction;
Stage #2: with water in tetrahydrofuran at 20; for 48 h;
References:
Pilkington-Miksa, Michael A.;Sarkar, Supti;Writer, Michele J.;Barker, Susie E.;Shamlou, Parviz Ayazi;Hart, Stephen L.;Hailes, Helen C.;Tabor, Alethea B. [European Journal of Organic Chemistry,2008,# 17,p. 2900 - 2914] Location in patent:experimental part