BENZYLHYDRAZINE DIHYDROCHLORIDE synthesis
1synthesis methods
- Product Name:BENZYLHYDRAZINE DIHYDROCHLORIDE
- CAS Number:20570-96-1
- Molecular formula:C7H10N2.2HCl
- Molecular Weight:195.09
Step 1: Tert-butyl hydrazinecarboxylate was reacted in acetone with MgSO4 and HOAc. The mixture was heated to reflux. After cooling and filtration, concentration gave a white solid (1).
Step 2: Compound (1) was dissolved in toluene with solid KOH and a
Step 2: Compound (1) was dissolved in toluene with solid KOH and a
561067-10-5
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20570-96-1
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Yield:-
Reaction Conditions:
with hydrogenchloride in tetrahydrofuran for 3 h;Heating;
References:
Meyer, Kevin G. [Synlett,2004,# 13,p. 2355 - 2356]