Bis(2-ethylhexyl)amine synthesis
- Product Name:Bis(2-ethylhexyl)amine
- CAS Number:106-20-7
- Molecular formula:C16H35N
- Molecular Weight:241.46
104-76-7
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104-75-6
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106-20-7
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Yield:-
Reaction Conditions:
with chlorocyclopentadienylbis(triphenylphosphine)ruthenium(II);urea;diphenylphosphinopropane in diethylene glycol dimethyl ether at 160; for 12 h;Autoclave;Inert atmosphere;
Steps:
2.3. General catalytic procedure for amination
General procedure: The autoclave was charged with 1-hexylalcohol (2.5 mmol) and urea (2.5 mmol) in 1mLdiglyme. [(Cp)RuCl(dppe)] (3percent mol) as catalyst, diphenylphosphinopropane (dppp)(0.07 mmol) as supporting ligand and 0.04 g K2CO3 as base was added. The autoclavewas closed, flushed with argon for 5 min and then temperature was adjusted at160 °C. After 12 h, the autoclave was cooled to room temperature and the productswere analyzed by gas chromatography.
References:
Dindar, Sara;Nemati Kharat, Ali [Journal of Coordination Chemistry,2020]
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106-20-7
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106-20-7
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106-20-7
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123-05-7
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106-20-7
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