ChemicalBook CAS DataBase List BIS(TRIMETHYLSILYL)CHLOROMETHANE

BIS(TRIMETHYLSILYL)CHLOROMETHANE synthesis

9synthesis methods

Product Name:BIS(TRIMETHYLSILYL)CHLOROMETHANE
CAS Number:5926-35-2
Molecular formula:C7H19ClSi2
Molecular Weight:194.85

a convenient one-pot procedure has been developed by Kemp and Cowley in which trimethylsilylchloride reacts with dichloromethane in the presence of nBuLi at ?110°Cto give bis(trimethylsilyl)dichloromethane.1 This intermediate is sequentially treated with nBuLi and ethanol to yield chlorobis(trimethylsilyl)methane. A number of other syntheses have been described

75-77-4
590 suppliers
$5.04/10

67-66-3 Synthesis

67-66-3
0 suppliers
$33.60/500ml

5926-38-5
46 suppliers
$79.40/5ml

5926-35-2
37 suppliers
$119.00/5g

15951-41-4
22 suppliers
$134.40/1G

Yield:5926-35-2 3% ，15951-41-4 3% ，5926-38-5 94%

Reaction Conditions:

with N,N,N,N-tetraethylammonium tetrafluoroborate in N,N-dimethyl-formamide; for 29.25 h;electroreduction, anode: Zn, cathode: stainless steel;

References:

Pons, P.;Biran, C.;Bordeau, M.;Dunogues, J. [Journal of Organometallic Chemistry,1988,vol. 358,p. 31 - 38]

15951-41-4
22 suppliers
$134.40/1G

5926-35-2
37 suppliers
$119.00/5g

41823-71-6
0 suppliers
inquiry

Lithium, [chlorobis(trimethylsilyl)methyl]-

27483-93-8
0 suppliers
inquiry

References

75-77-4
590 suppliers
$5.04/10

2344-80-1
296 suppliers
$15.00/1g

5926-35-2
37 suppliers
$119.00/5g

References

15951-41-4
22 suppliers
$134.40/1G

5926-35-2
37 suppliers
$119.00/5g

References

75-77-4
590 suppliers
$5.04/10

67-66-3 Synthesis

67-66-3
0 suppliers
$33.60/500ml

2117-28-4 Synthesis

2117-28-4
119 suppliers
$37.39/1g

5926-35-2
37 suppliers
$119.00/5g

1068-69-5
64 suppliers
$45.00/50mg

References

BIS(TRIMETHYLSILYL)CHLOROMETHANE Related Search:

1,3-DISILAPROPANE 1,3-DISILABUTANE Bis(trimethylsilyl)methane

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BIS(TRIMETHYLSILYL)CHLOROMETHANE synthesis

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