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ChemicalBook CAS DataBase List BOC-12-ADO-OH
18934-81-1

BOC-12-ADO-OH synthesis

3synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 3 steps
1: acetyl chloride / methanol / 2.25 h / 20 - 25 °C / Inert atmosphere
2: dmap; triethylamine / dichloromethane / 20 °C / Inert atmosphere
3: methanol; sodium hydroxide / 50 °C / Inert atmosphere

References:

GENSPERA, INC.;LYNCH, John K.;HUTCHISON, Jeffrey J.;Xiong Fu;Kevin Kunnen WO2014/145035, 2014, A1

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