Boric acid, tribenzyl ester synthesis
- Product Name:Boric acid, tribenzyl ester
- CAS Number:2467-18-7
- Molecular formula:C21H21BO3
- Molecular Weight:332.2
11113-50-1
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100-51-6
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2467-18-7
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$172.00/250mg
Yield:2467-18-7 88%
Reaction Conditions:
with calcium hydride in toluene;byproducts: H2; react. under N2, slow addn. of the alcohol via syringe to B(OH)3 (ratio 3:1) and CaH2, cooling in a water bath, slow heating to 80-90°C for 12 h after abating the H2 gas evolution; distn. of the volatile products under reduced pressure (distn. pot temp. <= 120°C), extn. with hot toluene or cyclohexane under N2;
References:
Cole, T. E.;Quintanilla, R.;Rodewald, S. [Synthesis and Reactivity in Inorganic and Metal-Organic Chemistry,1990,vol. 20,p. 55 - 64]
100-52-7
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2467-18-7
7 suppliers
$172.00/250mg
100-51-6
1398 suppliers
$5.00/100g
2467-18-7
7 suppliers
$172.00/250mg
93-58-3
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$14.00/25mL
2467-18-7
7 suppliers
$172.00/250mg
1694-84-4
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2467-18-7
7 suppliers
$172.00/250mg