BORON TRIFLUORIDE TERT-BUTYL METHYL ETHERATE synthesis
- Product Name:BORON TRIFLUORIDE TERT-BUTYL METHYL ETHERATE
- CAS Number:123334-27-0
- Molecular formula:C5H12BF3O
- Molecular Weight:155.96
16940-66-2
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$21.21/100ml
123334-27-0
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13755-29-8
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$6.00/25g
19287-45-7
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Yield:19287-45-7 >99 ，13755-29-8 93%
Reaction Conditions:
in further solvent(s);soln. NaBH4 in triglyme was added slowly for 3 h at room temp. to BF3-tert-butyl methyl etherate; B2H6 was absorbed with THF, NaBF4 was filtered off, solvent was removedby distillation to obtaine more NaBF4;
References:
Kanth, Josyula V. B.;Brown, Herbert C. [Inorganic Chemistry,2000,vol. 39,# 8,p. 1795 - 1802]