C-(4-METHOXY-PHENYL)-C-PHENYL-METHYLAMINE synthesis
- Product Name:C-(4-METHOXY-PHENYL)-C-PHENYL-METHYLAMINE
- CAS Number:2538-34-3
- Molecular formula:C14H15NO
- Molecular Weight:213.27
123-11-5
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2538-34-3
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Yield:2538-34-3 83%
Reaction Conditions:
Stage #1: 4-methoxy-benzaldehyde;phenylmagnesium bromidewith diphenyl phosphoryl azide in tetrahydrofuran;diethyl ether at 0 - 40; for 20 h;Schlenk technique;Inert atmosphere;
Stage #2: with lithium aluminium tetrahydride in tetrahydrofuran;diethyl ether at 0; for 1 h;Schlenk technique;Inert atmosphere;
References:
Goswami, Pratik P.;Suding, Victoria P.;Carlson, Angela S.;Topczewski, Joseph J. [European Journal of Organic Chemistry,2016,vol. 2016,# 28,p. 4805 - 4809] Location in patent:supporting information
100-66-3
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2538-34-3
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100-52-7
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2538-34-3
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5291-46-3
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2538-34-3
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$65.00/50mg