CYCLANDELATE synthesis
- Product Name:CYCLANDELATE
- CAS Number:456-59-7
- Molecular formula:C17H24O3
- Molecular Weight:276.37
Yield:-
Steps:
Multi-step reaction with 2 steps
1: dicyclohexyl-carbodiimide; dmap / dichloromethane / 0.33 h / 0 °C
2: cobalt(II) iodide; bis-diphenylphosphinomethane; sodium acetate; zinc; water / acetonitrile / 12 h / 80 °C / Inert atmosphere; Schlenk technique
References:
Gao, Yang;Zhang, Xuexin;Laishram, Ronibala Devi;Chen, Jingchao;Li, Kangkui;Zhang, Keyang;Zeng, Guangzhi;Fan, Baomin [Advanced Synthesis and Catalysis,2019,vol. 361,# 17,p. 3991 - 3997]
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