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ChemicalBook CAS DataBase List Cyclohexanol, 1-(2-bromophenyl)-
255837-16-2

Cyclohexanol, 1-(2-bromophenyl)- synthesis

1synthesis methods
-

Yield:255837-16-2 70%

Reaction Conditions:

Stage #1: 2,3-dibromobenzenewith n-butyllithium in tetrahydrofuran;diethyl ether;hexane at -110; for 1.75 h;Inert atmosphere;
Stage #2: cyclohexanone in tetrahydrofuran;diethyl ether;hexane at -110 - 20; for 13 h;Inert atmosphere;

References:

Kinoshita, Hidenori;Hirai, Nobuyoshi;Miura, Katsukiyo [Journal of Organic Chemistry,2014,vol. 79,# 17,p. 8171 - 8181]

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