Cyclohexanone, 2-(3-methylphenyl)- synthesis
- Product Name:Cyclohexanone, 2-(3-methylphenyl)-
- CAS Number:32045-66-2
- Molecular formula:C13H16O
- Molecular Weight:188.27
93429-59-5
5 suppliers
inquiry
32045-66-2
5 suppliers
inquiry
Yield:32045-66-2 79%
Reaction Conditions:
Stage #1: trans-2-(3-methylphenyl)cyclohexan-1-olwith oxalyl dichloride;dimethyl sulfoxide in dichloromethane at -78; for 0.333333 h;Inert atmosphere;
Stage #2: with triethylamine in dichloromethane at -78 - 20; for 0.583333 h;Inert atmosphere;
References:
Duong, Hung A.;Gilligan, Ruth E.;Cooke, Michael L.;Phipps, Robert J.;Gaunt, Matthew J. [Angewandte Chemie - International Edition,2011,vol. 50,# 2,p. 463 - 466] Location in patent:supporting information; experimental part
286-20-4
211 suppliers
$15.00/25g
32045-66-2
5 suppliers
inquiry
121905-60-0
41 suppliers
inquiry
32045-66-2
5 suppliers
inquiry