Cyclohexanone, 4-(1-methylethenyl)- synthesis
- Product Name:Cyclohexanone, 4-(1-methylethenyl)-
- CAS Number:22460-53-3
- Molecular formula:C9H14O
- Molecular Weight:138.21
![Silane, trimethyl[[4-(1-methylethenyl)-1-cyclohexen-1-yl]oxy]-, (S)- (9CI)](/CAS/20210111/GIF/145747-47-3.gif)
145747-47-3
0 suppliers
inquiry
22460-53-3
1 suppliers
inquiry
Yield:-
Reaction Conditions:
with HF in dichloromethane;water;trimethylamine;
Steps:
7 4-Isopropenylcyclohexanone
4-Isopropenylcyclohexanone 4.1 g of a 37% strength solution of HF in trimethylamine were added dropwise with stirring at room temperature to 8.0 g (0.038 mol) of 1-trimethylsilyloxy-4-isopropenyl-1-cyclohexene in 100 ml of CH2 Cl2, and the mixture was subsequently stirred for 2 hours. Water was added, extraction was carried out with CH2 Cl21 and the combined organic phases were dried and concentrated. 4.7 g (90% of theory) were obtained of a colorless oil which was reacted without further purification.
References:
US5889012,1999,A
18031-40-8
237 suppliers
$6.00/1g
22460-53-3
1 suppliers
inquiry
![1,4-Dioxaspiro[4.5]decane, 8-(1-methylethenyl)-](/CAS/20210111/GIF/70850-38-3.gif)
70850-38-3
13 suppliers
inquiry
22460-53-3
1 suppliers
inquiry
