Decahydronaphthalene synthesis
- Product Name:Decahydronaphthalene
- CAS Number:91-17-8
- Molecular formula:C10H18
- Molecular Weight:138.25
90-15-3
741 suppliers
$9.00/5g
119-64-2
350 suppliers
$9.00/25g
529-35-1
133 suppliers
$9.00/1g
91-17-8
289 suppliers
$10.00/5mL
Yield:529-35-1 71.8%
Reaction Conditions:
with hydrogen in methanol at 80; under 22502.3 Torr; for 4 h;Catalytic behavior;Autoclave;chemoselective reaction;Temperature;Pressure;Reagent/catalyst;
Steps:
Reaction procedure
Hydrogenation reactions were carried out in a 100-ml high-pressure stainless-steel autoclave. A weighed amount of catalyst, reactant, and methanol solvent were placed in the autoclave and flushed three times with nitrogen. After the required temperature had been attained, hydrogen was regulated at certain pressure and introduced into the reactor. The reaction was carried out for certain time at constant temperature and hydrogen pressure. After reaction completion, the reactor was cooled down. The pressure was released slowly, and the contents were identified by gas chromatography-mass spectrometry (GC-MS; HP5890 GC-HP5971 MSD) and quantitatively analyzed by GC-flame ionization detector (FID). For both GC instruments, the column was a 30 m x 0.25 mm i.d. HP-5 capillary column.
References:
Wang, Bo;Liu, Hui [Research on Chemical Intermediates,2017,vol. 43,# 5,p. 3197 - 3204]
91-20-3
527 suppliers
$14.00/25g
91-17-8
289 suppliers
$10.00/5mL
119-64-2
350 suppliers
$9.00/25g
91-17-8
289 suppliers
$10.00/5mL
90-15-3
741 suppliers
$9.00/5g
119-64-2
350 suppliers
$9.00/25g
529-35-1
133 suppliers
$9.00/1g
529-34-0
475 suppliers
$6.00/10g
91-17-8
289 suppliers
$10.00/5mL