DI-N-HEXYL SULFONE synthesis
- Product Name:DI-N-HEXYL SULFONE
- CAS Number:16823-61-3
- Molecular formula:C12H26O2S
- Molecular Weight:234.4
6294-31-1
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Yield:16823-61-3 99%
Reaction Conditions:
with phthalic anhydride;urea hydrogen peroxide adduct in ethyl acetate at 20;Green chemistry;
Steps:
Procedure B:
General procedure: To a solution of sulfide 1 (200 mg, 1-2 mmol, 1 equiv) in EtOAc (5 mL) was added UHP (3 equiv) and phthalic anhydride (3equiv) and the solution was allowed to stir for 12-16 h at r.t. The reaction was quenched with sat. aq Na2SO3 (10 mL) and then diluted withEtOAc (5 mL). The organics were washed with 1 N aq NaOH (2 × 10mL), H2O (10 mL), and brine (10 mL). The organics were dried (Na2-SO4) and concentrated to give the desired, spectroscopically pure sulfoneproduct.
References:
Lutz, Marlon;Wenzler, Marta;Likhotvorik, Igor [Synthesis,2018,vol. 50,# 11,p. 2231 - 2234] Location in patent:supporting information
111-25-1
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111-31-9
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