DBCO-amine synthesis
- Product Name:DBCO-amine
- CAS Number:1255942-06-3
- Molecular formula:C18H16N2O
- Molecular Weight:276.33
2222-33-5
329 suppliers
$6.00/5g
1255942-06-3
197 suppliers
$51.60/10mg
Yield:-
Steps:
Multi-step reaction with 7 steps
1: hydroxylamine hydrochloride / pyridine / 20 h / Reflux
2: polyphosphoric acid / 1 h / 125 °C
3: lithium aluminium tetrahydride / diethyl ether / 15 h / Reflux
4: pyridine / dichloromethane / 0.5 h / 20 °C
5: pyridinium perbromide hydrobromide / dichloromethane / 20 °C
6: potassium tert-butylate / tetrahydrofuran / 1 h / 20 °C
7: potassium carbonate / methanol; water / 20 °C
References:
Kuzmin, Alexander;Poloukhtine, Andrei;Wolfert, Margreet A.;Popik, Vladimir V. [Bioconjugate Chemistry,2010,vol. 21,# 11,p. 2076 - 2085]
![dibenzo[b,f]azocin-6(5H)-one](/CAS/20180703/GIF/23112-88-1.gif)
23112-88-1
52 suppliers
inquiry
1255942-06-3
197 suppliers
$51.60/10mg
![(Z)-5,6-dihydrodibenzo[b,f]azocine](/CAS/20200119/GIF/23194-93-6.gif)
23194-93-6
83 suppliers
$125.00/100mg
1255942-06-3
197 suppliers
$51.60/10mg
![5H-dibenzo[a,d]cyclohepten-5-one oxime](/CAS/GIF/1021-91-6.gif)
1021-91-6
43 suppliers
$33.00/100mg
1255942-06-3
197 suppliers
$51.60/10mg